B006874 - ORGANIC CHEMISTRY LABORATORY I

italian

Italian

This course aims to teach the techniques basic to organic chemistry laboratory. At the end of the course the students will be able to run simple experiments and reactions of organic chemistry. Safety issues, glassware and equipment, main purification techniques of organic compounds and how to make laboratory notebooks and laboratory reports will be illustrated, as well as the basic principle of IR and NMR spectroscopy.

This course aims to teach the techniques basic to organic chemistry laboratory. At the end of the course the students will be able to run simple experiments and reactions of organic chemistry. Safety issues, glassware and equipment, main purification techniques of organic compounds and how to make laboratory notebooks and laboratory reports will be illustrated, as well as the basic principle of IR and NMR spectroscopy.

1) L.M. Harwood, C.J.Moody, J.M. Percy EXPERIMENTAL ORGANIC CHEMISTRY Standard and Microscale - Blackwell Science ed. (2) R.M. Roberts, J.C. Gilbert, S.F. Martin CHIMICA ORGANICA SPERIMENTALE - Zanichelli ed. (3) L.D. Field, S. Sternhell, J.R. Kalman ORGANIC STRUCTURES FROM SPECTRA - John Wiley & Sons ed. L.M. Harwood, C.J.Moody, J.M. Percy EXPERIMENTAL ORGANIC CHEMISTRY Standard and Microscale Blackwell Science ed. R.M. Roberts, J.C. Gilbert, S.F. Martin CHIMICA ORGANICA SPERIMENTALE Zanichelli ed. L.D. Field, S. Sternhell, J.R. Kalman ORGANIC STRUCTURES FROM SPECTRA John Wiley & Sons ed.

1) L.M. Harwood, C.J.Moody, J.M. Percy EXPERIMENTAL ORGANIC CHEMISTRY Standard and Microscale - Blackwell Science ed. (2) R.M. Roberts, J.C. Gilbert, S.F. Martin CHIMICA ORGANICA SPERIMENTALE - Zanichelli ed. (3) L.D. Field, S. Sternhell, J.R. Kalman ORGANIC STRUCTURES FROM SPECTRA - John Wiley & Sons ed. L.M. Harwood, C.J.Moody, J.M. Percy EXPERIMENTAL ORGANIC CHEMISTRY Standard and Microscale Blackwell Science ed. R.M. Roberts, J.C. Gilbert, S.F. Martin CHIMICA ORGANICA SPERIMENTALE Zanichelli ed. L.D. Field, S. Sternhell, J.R. Kalman ORGANIC STRUCTURES FROM SPECTRA John Wiley & Sons ed.

Students learn the principles of the main manual and instrumental techniques aimed to purify the organic compounds, and the basic principles of IR and NMR spectroscopy. Students learn how to behave safely in an organic chemistry laboratory and how to prevent any risk due to hazards linked to exposure to toxic/inflammable substances. Students also learn how to work in small groups. Student learn how to carry out simple organic reactions and to purify the obtained products. They also learn how to use instrumentation for the analysis of the physical-chemical properties of compounds (HPLC, GC, IR, mp)

Students learn the principles of the main manual and instrumental techniques aimed to purify the organic compounds, and the basic principles of IR and NMR spectroscopy. Students learn how to behave safely in an organic chemistry laboratory and how to prevent any risk due to hazards linked to exposure to toxic/inflammable substances. Students also learn how to work in small groups. Student learn how to carry out simple organic reactions and to purify the obtained products. They also learn how to use instrumentation for the analysis of the physical-chemical properties of compounds (HPLC, GC, IR, mp)

Courses required: Organic Chemistry I

Courses recommended: General and Inorganic Chemistry, General and Inorganic Chemistry Lab.

Courses required: Organic Chemistry I

Courses recommended: General and Inorganic Chemistry, General and Inorganic Chemistry Lab.

Contact hours for: Lectures (hours): 16
Contact hours for: Laboratory (hours): 48

Contact hours for: Lectures (hours): 16
Contact hours for: Laboratory (hours): 48

No additional info

Written examination.

Written examination aimed at assessing the ability of the student to assign the structure of an organic compound through spectroscopic techniques, as well as to establish a practical protocol for its preparation in laboratory.

Security in the lab. Glassware, notebook and lab-report. TLC and GC. Work up procedures. Crystallisation, distillation and column chromatography. Characterisation of compounds (mp, bp). IR spectroscopy. NMR spectroscopy. Nomenclature, stereochemistry and conformational analysis of organic compounds.

Security in the lab. Glassware, notebook and lab-report. TLC and GC. Work up procedures. Crystallisation, distillation and column chromatography. Characterisation of compounds (mp, bp). HPLC chromatography. IR spectroscopy. NMR spectroscopy. Names, stereochemistry and conformational analysis of organic compounds.